Allene Synthesis from 2-Alkyn-1-Ols
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https://doi.org/10.1016/S0040-4039(00)76187-9Metadata
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Myers, Andrew G., Nathaniel S. Finney, and Elaine Y. Kuo. 1989. Allene synthesis from 2-alkyn-1-Ols. Tetrahedron Letters 30(42): 5747-5750.Abstract
Activation of 2-alkyn-1-01s as their methanesulfonate esters and displacement with hydrazine urnishes the corresponding alkynyl hydrazine derivatives which undergo smooth oxidative rearrangement with diethyl azodicarboxylate (DEAD) or 4-methyl-1,2,4-triazoline-3,5-dione (MTAD) to form allenes.Citable link to this page
http://nrs.harvard.edu/urn-3:HUL.InstRepos:3122543
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