Allene Synthesis from 2-Alkyn-1-Ols

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Allene Synthesis from 2-Alkyn-1-Ols

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Title: Allene Synthesis from 2-Alkyn-1-Ols
Author: Kuo, Elaine Y.; Finney, Nathaniel S.; Myers, Andrew

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Citation: Myers, Andrew G., Nathaniel S. Finney, and Elaine Y. Kuo. 1989. Allene synthesis from 2-alkyn-1-Ols. Tetrahedron Letters 30(42): 5747-5750.
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Abstract: Activation of 2-alkyn-1-01s as their methanesulfonate esters and displacement with hydrazine urnishes the corresponding alkynyl hydrazine derivatives which undergo smooth oxidative rearrangement with diethyl azodicarboxylate (DEAD) or 4-methyl-1,2,4-triazoline-3,5-dione (MTAD) to form allenes.
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