Allene Synthesis from 2-Alkyn-1-Ols
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Finney, Nathaniel S.
Kuo, Elaine Y.
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CitationMyers, Andrew G., Nathaniel S. Finney, and Elaine Y. Kuo. 1989. Allene synthesis from 2-alkyn-1-Ols. Tetrahedron Letters 30(42): 5747-5750.
AbstractActivation of 2-alkyn-1-01s as their methanesulfonate esters and displacement with hydrazine urnishes the corresponding alkynyl hydrazine derivatives which undergo smooth oxidative rearrangement with diethyl azodicarboxylate (DEAD) or 4-methyl-1,2,4-triazoline-3,5-dione (MTAD) to form allenes.
Citable link to this pagehttp://nrs.harvard.edu/urn-3:HUL.InstRepos:3122543
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