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Using Magnetic Levitation to Separate Mixtures of Crystal Polymorphs

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2013

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10.1002/ange.201305549

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Wiley-VCH Verlag Berlin
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Atkinson, Manza B. J., David K. Bwambok, Jie Chen, Prashant D. Chopade, Martin M. Thuo, Charles R. Mace, Katherine A. Mirica, Ashok A. Kumar, Allan S. Myerson, and George M. Whitesides. 2013. “Using Magnetic Levitation to Separate Mixtures of Crystal Polymorphs.” Angewandte Chemie 125(39): 10398–10401.

Abstract

Magnetische Levitation (MagLev) ist eine einfache Trennmethode für Kristallpolymorphe mit Dichteunterschieden (Δρ) von nur 0.001 g cm−3. Für vier organische Verbindungen wurden dichtebasierte Trennungen verschiedener kristalliner Formen gezeigt: 5-Methyl-2-[(2-nitrophenyl)amino]-3-thiophencarbonitril, Sulfathiazol, Carbamazepin und trans-Zimtsäure.

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Dichte; Kristallpolymorphe; Kristallwachstum; Magnetische Eigenschaften; Paramagnetische Lösungen

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http://nrs.harvard.edu/urn-3:HUL.InstRepos:12361262

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