Publication: Gram-Scale Synthesis of the A′B′-Subunit of Angelmicin B
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Date
2011
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American Chemical Society (ACS)
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Milgram, Benjamin C., Brian B. Liau, and Matthew D. Shair. 2011. “Gram-Scale Synthesis of the A′B′-Subunit of Angelmicin B.” Organic Letters 13 (24) (December 16): 6436–6439. doi:10.1021/ol202728v.
Abstract
A gram-scale enantiospecific synthesis of the A’B’-subunit of angelmicin B is reported. The synthesis involves a Lewis acid-catalyzed contrasteric Diels–Alder reaction and a tandem silyl zincate 1,6-addition/enolate oxidation sequence.
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