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Synthesis of Oxazocenones via Gold(I)-Catalyzed 8-Endo-Dig Hydroalkoxylation of Alkynamides

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2015

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American Chemical Society
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Scully, Stephen S., Shao-Liang Zheng, Bridget K. Wagner, and Stuart L. Schreiber. 2015. “Synthesis of Oxazocenones via Gold(I)-Catalyzed 8-Endo-Dig Hydroalkoxylation of Alkynamides.” Organic Letters 17 (3): 418-421. doi:10.1021/ol503273v. http://dx.doi.org/10.1021/ol503273v.

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Abstract

Several benzoxazocenones have been found to exhibit novel cellular activities. In the present study, we report a gold(I)-catalyzed 8-endo-dig hydroalkoxylation reaction of alkynamides to access analogous oxazocenone scaffolds. This methodology provided an advanced intermediate, which was elaborated to a des-benzo analog of a bioactive benzoxazocenone.

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